Read e-book online Solid-State NMR: Basic Principles and Practice PDF

By David C. Apperley,Robin K. Harris,Paul Hodgkinson

the facility of nuclear magnetic resonance, NMR, for characterizing molecules dissolved in answer is broadly said and NMR varieties a vital part of undergraduate chemistry levels. notwithstanding, the applying of NMR to the forged kingdom is way much less good favored. this article units out the basic ideas of solid-state NMR, explaining how NMR in solids differs from that during answer, displaying how a few of the interactions of NMR could be manipulated to yield high-resolution spectra and to provide details on neighborhood constitution and dynamics in solids. This publication goals to take a few of the mystique out of solid-state NMR via supplying a understandable dialogue of the technique, together with the fundamental thoughts and a realistic advisor to implementation of the experiments. A uncomplicated wisdom of solution-state NMR is thought and is just in brief lined. The textual content is meant for these in academia and anticipating to exploit solid-state NMR of their study and searching out an available creation to the sector. it is going to even be precious for non-experts attracted to studying how NMR might be usefully utilized to sturdy platforms. specified mathematical remedies are behind schedule to a bankruptcy on the mid-point of the textual content and will be skipped. Introductions to experiments and numerical simulations are supplied to aid hyperlink NMR effects to experimental perform. different elements of solid-state NMR, from uncomplicated pulse-and-acquire experiments to stylish recommendations for the size of anisotropy info are provided. Examples illustrate the big variety of purposes of the procedure and its complementarity to different solid-state characterization thoughts corresponding to X-ray diffraction. numerous elements of NMR crystallography are coated as are themes of movement in solids.

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Solid-State NMR: Basic Principles and Practice by David C. Apperley,Robin K. Harris,Paul Hodgkinson


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