Neuartige Ylidinkomplexe des Niobs: Synthese und Reaktionen by David Hoffmann PDF

By David Hoffmann

David
Hoffmann stellt die Synthese der ersten Niobtetrelylidinkomplexe des Germaniums
und Zinns durch effiziente Salzmetathesereaktion vor. Beide Verbindungen wurden
vom Autor IR- und Multikern‑NMR‑spektroskopisch charakterisiert und ihre
Molekülstruktur im Festkörper durch Röntgenstrahlenbeugung am Einkristall
aufgeklärt und diskutiert. Beide Strukturen weisen einen sehr kurzen
Tetrel-Niob-Bindungsabstand und ein quickly linear koordiniertes Tetrelatom auf. Die
Reaktivität des Niobgermylidinkomplexes gegenüber kleinen polaren Molekülen wurde
anhand der Reaktionen mit Methanol und Wasser geprüft und die Redoxeigenschaften
mittels cyclovoltammetrischer Messungen untersucht.

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Neuartige Ylidinkomplexe des Niobs: Synthese und Reaktionen (BestMasters) (German Edition) by David Hoffmann


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